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Impedance Camera to observe impedance evolution in time

Time-Resolved Impedance Spectroscopy, entire frequency spectrum in a single shot.

description

The instrument is designed for the Time-Resolved Impedance Spectroscopy. Typically, when Impedance Spectroscopy measurements are performed, impedance of a sample is measured subsequently for each frequency applied. However, if a dynamically changing sample is examined, its properties may significantly change during the frequency sweep. A resulted impedance spectrum might be hard to interpret in such a case. The Impedance Camera takes an entire frequency spectrum with selectable sweep limits in a single shot. All the frequencies are handled at the same time. To observe the time evolution of a sample, many frames may be recorded with a given time interval. The instrument enables to investigate the dynamics of different types of samples, such as electrochemical sensors, materials that changes its properties when exposed to a given agent (light, temperature, catalyst, etc.) and others.

Instrument measures current flowing through the sample and voltage on the sample in response to a voltage signal generated as a superposition of frequencies.

The measurement results are presented in:

    • 3D Nyquist (Argand) plot in time,
    • Bode plots in time,
    • Time evolution plot of an impedance at a given frequency contained in generated signal,
    • Difference plots to observe relative changes in time,
    • Plots with raw current and raw voltage frames collected.

The camera is ideal to observe the real time impedance development of electrochemical sensors.
The Impedance Camera enables to conduct experiments that are  complementary to  static photocurrent/photovoltage measurements  performed, for example, with Photoelectric Spectrometer or a Mini Photoelectric Spectrometer.

device modules

The instrument consists of:

  • Measurement electronics module
  • Measurement head: Basic/Electrochemical,
  • 12 V power supply,
Click to enlarge

 

Impedance Camera for electrochemical measurements

Impedance Camera combined with the Electrochemical Head and the Sample Chamber serves as a measurement setup dedicated for the electrochemical samples that needs to be screened from the ambient light and external EM fields.

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specifications

Impedance Camera

  • Number of frames in a sequence: unlimited,
  • Number of frequencies in a frame: unlimited,
  • Range of generated potential signal: -1 ÷ 1 V,
  • Measurement Head types: Basic (Two-Electrode)/Electrochemical (Three-Electrodes),
  • Sampling rates: 1.22 kHz ÷ 10 MHz,

Basic Head

  • Current ranges: 10 mA, 1 mA,
  • Frequency ranges: 1mHz ÷ 1 MHz,

Electrochemical Head

  • Current ranges: 1 mA, 100 μA, 10 μA, 1 μA, 100 nA, 10 nA,
  • Bandwidth ranges: 2.5 MHz, 1.3 MHz, 300 kHz, 35 kHz, 3kHz, 300 Hz,
exemplary results

The measurement results shown below are obtained for a parallel RC circuit where the resistance was depends on the oscillating illumination intensity.

Nyquist (or Argand) plot presents a real and imaginary part of impedance measured for range of frequencies at various times. One can see the impedance value increases in the middle of the measuring sequence and the impedance semicircles grow in the diameter.
The green color selects the same frequency measurement points in time. If only capacitance was changed, in the RC circuit, all semicircles would be the same size but position of given frequency points would move along a circle.
Click to enlarge

A single frame 3D Nyquist (Argand) plot.
Click to enlarge

Bode plots amplitudes in time.
Click to enlarge

Bode plots phases in time.
Click to enlarge

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